HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Butanesulfonyl chloride → HCID 57883686, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Butanesulfonyl chloride | HCID 75430 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | HCID 86761257 | HCID 86761257 | — |
| Product | HCID 57883686 | HCID 57883686 | 61% |
Reaction Steps
Prepared as described in general procedure (Q) using 1,1-dicyclohexyl-3-(5-piperazin-1-ylmethyl-thiazol-2-yl)-urea hydrochloride (30 mg, 0.06 mmol), DIEA (32 μL, 0.18 mmol) and butane-1-sulfonyl chloride (16 μL, 0.12 mmol) to afford 19 mg (61%) of the desired product after purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07872139B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-449ee115dbc342aaadf03e106ac129f7 |
| Source note | uspto-grants-2011_01 |