HCID 86619097, compound → HCID 86619098, compound

Participants

Reaction Steps

tert-butyl N2-[(benzyloxy)carbonyl]-N5-(tert-butoxycarbonyl)-D-ornithinate (0.67 g, 1.83 mmole) and Pd on charcoal (95%, 0.115 g) were mixed in EtOH (95%, 20 mL) and stirred under H2-atmosphere for 5 hours and 15 minutes. The mixture was filtered through Celite 521 and the solvent was evaporated under reduced pressure to give 0.45 g (85%) of the desired product.

Provenance & Evidence