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tert-Butyl pentanoate → HCID 178444126、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | tert-Butyl pentanoate | HCID 520048 | — |
| 反応物 | HCID 178436316 | HCID 178436316 | — |
| 生成物 | HCID 178444126 | HCID 178444126 | 93.2% |
反応手順
Reaction operations were carried out according to the first step of Example 1 by using 2-(trans-4-(4-ethylphenyl)cyclohexyl)oxetane (42) (7.5 g, 30.9 mmol) and tert-butyl pentanoate (43) (15.6 g, 98.9 mmol) as starting materials to obtain tert-butyl 2-propyl-5-hydroxy-5-(trans-4-(4-ethylphenyl)cyclohexyl)pentanoate (44) (11.6 g, 28.8 mmol). The yield based on the compound (42) was 93%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07875327B2 |
| 出典データセット | uspto-grants-2011_01 |
| ORD ID | ord-6d3d2ac61f334cb58521a34cb0c6da8e |
| 出典メモ | uspto-grants-2011_01 |