HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → 1-Bromo-8-fluoro-3,4-dimethylimidazo[1,5-a]quinoxaline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | 8-Fluoro-3,4-dimethylimidazo[1,5-a]quinoxaline | HCID 57732459 | — |
| Product | 1-Bromo-8-fluoro-3,4-dimethylimidazo[1,5-a]quinoxaline | HCID 57732452 | 89% |
Reaction Steps
Reaction of intermediate 4A (1.55 g, 7.2 mmol) and NBS (1.92 g, 10.8 mmol) provided the product 5A as an off-white solid (1.87 g, 89% yield). EIMS 293.9 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07875618B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-2870e4b00688498ab67c8c12701b213e |
| Source note | uspto-grants-2011_01 |