HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 254317Generated: November 1, 2026
Dimethylformamide → 1-(2-Chlorophenyl)-3,4-dimethyl-7-(3-nitrobenzyloxy)-imidazo(1,5-a)quinoxaline
https://huagongshe.com/reaction/254317
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | Benzene, 1-(bromomethyl)-3-nitro- | HCID 77568 | — |
| Reactant | HCID 42629710 | HCID 42629710 | — |
| Solvent | Water | HCID 962 | — |
| Product | 1-(2-Chlorophenyl)-3,4-dimethyl-7-(3-nitrobenzyloxy)-imidazo(1,5-a)quinoxaline | HCID 42629830 | — |
Reaction Steps
1.5 g 1-(2-Chloro-phenyl)-3,4-dimethyl-7-hydroxy-imidazo(1,5-a)quinoxaline, 3.36 g Caesium carbonate, 80 mL N,N-dimethylformamide, and 9 mL water were stirred for 10 min followed by addition of 1.3 g 3-nitro-benzylbromide. After 3 h stirring at 120° C. the reaction mixture was given into 250 mL water, filtered off, washed with water, dried under reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07875618B2 |
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| Source dataset | uspto-grants-2011_01 |
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| ORD ID | ord-44a65d42130c4c5c9da490663afcfc22 |
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| Source note | uspto-grants-2011_01 |
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