Phosphorus tribromide → HCID 58951777, compound

HRID 254490Notes

Reaction equation

[F:1][C:2]1[C:7]([F:8])=[CH:6][CH:5]=[CH:4][C:3]=1[CH:9](O)[CH2:10][CH3:11].P(Br)(Br)[Br:14]>>[Br:14][CH:9]([C:3]1[CH:4]=[CH:5][CH:6]=[C:7]([F:8])[C:2]=1[F:1])[CH2:10][CH3:11]

Participants

Reactant 2

HCID 24614Phosphorus tribromide

HCID 11105813HCID 11105813, compound

Product 1

HCID 58951777HCID 58951777, compound

Procedure

rac-1-(1-Bromo-propyl)-2,3-difluoro-benzene was prepared from rac-1-(2,3-Difluoro-phenyl)-propan-1-ol and phosphorus tribromide in analogy to Example 23 b): colourless oil.

Sources & evidence

ORD record: ord-87a468c947f2442cbf9b5e20c7cc193e
Source dataset: uspto-grants-2011_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07875645B2

Reaction notes

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