Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
p-Toluenesulfonic acid → HCID 178448985, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | p-Toluenesulfonic acid | HCID 6101 | — |
| 반응물 | Butylamine | HCID 8007 | — |
| 반응물 | 2,3-Dichloro-6-fluorobenzaldehyde | HCID 3260062 | — |
| 생성물 | HCID 178448985 | HCID 178448985 | — |
반응 단계
Butyl-[1-(2,3-dichloro-6-fluoro-phenyl)-meth-(E)-ylidene]-amine was prepared from 2,3-dichloro-6-fluorobenzaldehyde, N-butylamine and p-toluenesulphonic acid in analogy to Example 191a): brown oil; 1H-NMR (CDCl3): 0.96 (3H, t, CH3), 1.39 (2H, sextet, CH2), 1.73 (2H, quintet, CH2), 3.71 (2H, q, CH2), 7.02 (1H, dd, ArH), 7.44 (1H, dd, ArH), 8.44 (1H, s, CH═N).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07875645B2 |
| 출처 데이터셋 | uspto-grants-2011_01 |
| ORD ID | ord-3eb247a4e17f4391855299c2a1d48fa7 |
| 출처 메모 | uspto-grants-2011_01 |