HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon tetrabromide → HCID 58951753, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon tetrabromide | HCID 11205 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | HCID 58951745 | HCID 58951745 | — |
| Product | HCID 58951753 | HCID 58951753 | — |
Reaction Steps
1-Chloro-3-(2,2-dibromo-vinyl)-2,4-diethyl-benzene was prepared from 3-chloro-2,6-diethyl-benzaldehyde, carbon tetrabromide and triphenylphosphine in analogy to Example 1d): colourless oil; 1H-NMR (CDCl3): 1.14 (3H, t, CH3), 1.17 (3H, t, CH3), 2.56 (2H, qd, CH2), 2.72 (2H, q, CH2), 7.03 (1H, d, ArH), 7.29 (1H, d, ArH), 7.44 (1H, s, CH═CBr2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07875645B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-e8245555966241e9b2688dd0cba253ef |
| Source note | uspto-grants-2011_01 |