Ethylenediamine → HCID 24779849, compound
Reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][CH3:9])=[C:4]([CH:10]=[C:11](Br)Br)[C:3]=1[CH2:14][CH3:15].[CH2:16]([NH2:19])[CH2:17][NH2:18]>>[Cl:1][C:2]1[C:3]([CH2:14][CH3:15])=[C:4]([C:5]([CH2:8][CH3:9])=[CH:6][CH:7]=1)[CH2:10][C:11]1[NH:18][CH2:17][CH2:16][N:19]=1Participants
3
Procedure
2-(3-Chloro-2,6-diethyl-benzyl)-4,5-dihydro-1H-imidazole was prepared from 1-chloro-3-(2,2-dibromo-vinyl)-2,4-diethyl-benzene and ethylenediamine in analogy to Example 1e): yellow crystals; MS (ISP): 251.3 ([M+H]+, 100%).
Sources & evidence
- ORD record
- ord-78860e97940c46e7bf9622d6ff3239dd
- Source dataset
- uspto-grants-2011_01
- Patent number
- US07875645B2
Reaction notes
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