HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon tetrabromide → HCID 58951868, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon tetrabromide | HCID 11205 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | HCID 58951814 | HCID 58951814 | — |
| Product | HCID 58951868 | HCID 58951868 | — |
Reaction Steps
2-(2,2-Dibromo-vinyl)-1,3-diethyl-4-fluoro-benzene was prepared from 2,6-diethyl-3-fluoro-benzaldehyde, carbon tetrabromide and triphenylphosphine in analogy to Example 1d): colourless oil; 1H-NMR (CDCl3): 1.15 (3H, t, CH3), 1.18 (3H, t, CH3), 2.58 (4H, m, 2×CH2), 6.97 (1H, dd, ArH), 7.04 (1H, dd, ArH), 7.42 (1H, s, CH═CBr2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07875645B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-43f904cacfc443ad9e5eb18b2df34394 |
| Source note | uspto-grants-2011_01 |