HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylacetate heptane → 3-Chloro-2-ethyl-6-fluoro-benzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylacetate heptane | HCID 21899848 | — |
| Reactant | HCID 178448984 | HCID 178448984 | — |
| Product | 3-Chloro-2-ethyl-6-fluoro-benzaldehyde | HCID 58951706 | — |
Reaction Steps
3-Chloro-2-ethyl-6-fluoro-benzaldehyde was prepared from butyl-[1-(3-chloro-2-ethyl-6-fluoro-phenyl)-meth-(E)-ylidene]-amine by flash chromatography (silica gel, ethyl acetate/heptane gradient): yellow oil; 1H-NMR (CDCl3): 1.21 (3H, t, CH3), 3.16 (2H, q, CH2), 6.99 (1H, dd, ArH), 7.55 (1H, dd, ArH), 10.45 (1H, s, CH═O).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07875645B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-e6b228def1684e38b3c48f8f42681868 |
| Source note | uspto-grants-2011_01 |