HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylenediamine → 2-(3-Chloro-2-ethyl-6-fluoro-benzyl)-4,5-dihydro-1H-imidazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylenediamine | HCID 3301 | — |
| Reactant | 1-Chloro-3-(2,2-dibromo-vinyl)-2-ethyl-4-fluoro-benzene | HCID 58951798 | — |
| Product | 2-(3-Chloro-2-ethyl-6-fluoro-benzyl)-4,5-dihydro-1H-imidazole | HCID 24779850 | — |
Reaction Steps
2-(3-Chloro-2-ethyl-6-fluoro-benzyl)-4,5-dihydro-1H-imidazole was prepared from 1-chloro-3-(2,2-dibromo-vinyl)-2-ethyl-4-fluoro-benzene and ethylenediamine in analogy to Example 1e): yellow crystals; MS (ISP): 243.3 ([M+H]+, 30%), 241.2 ([M+H]+, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07875645B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-4a5f4a20acc348a3ba3572a006da0004 |
| Source note | uspto-grants-2011_01 |