Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 254580Generated: October 29, 2026

Carbon tetrabromide → HCID 58951695, compound

https://huagongshe.com/reaction/254580

Reaction equation

Participants

RoleNameHCIDCharge
ReactantCarbon tetrabromideHCID 11205—
ReactantTriphenylphosphineHCID 11776—
ReactantHCID 58951904HCID 58951904—
ProductHCID 58951695HCID 58951695—

Reaction Steps

2-(2,2-Dibromo-vinyl)-1,3-diethyl-4-methoxy-benzene was prepared from 2,6-diethyl-3-methoxy-benzaldehyde, carbon tetrabromide and triphenylphosphine in analogy to Example 1d): colourless oil; 1H-NMR (CDCl3): 1.08 (3H, t, CH3), 1.17 (3H, t, CH3), 2.55 (4H, m, 2×CH2), 3.81 (3H, s, OMe), 6.82 (1H, d, ArH), 7.05 (1H, d, ArH), 7.44 (1H, s, CH═CBr2).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07875645B2
Source datasetuspto-grants-2011_01
ORD IDord-3728eeb98edb49779f63e822b7855f2d
Source noteuspto-grants-2011_01