Methanol → HCID 86605272, compound

Participants

Reaction Steps

To a solution of the amine 57 (16.2 mmol) in methanol (55 ml), was added phthalic anhydride (216.2 mmol), and the whole stirred for 2 h. The mixture was then evaporated to dryness under reduced pressure and the residue azeotroped with toluene to leave a cream solid 58.

Provenance & Evidence