1-Adamantanecarboxylic acid → HCID 66859715, compound

Participants

Reaction Steps

The product of Example 58A (0.11 g, 0.49 mmol) and adamantane-1-carboxylic acid (97 mg, 0.54 mmol) were processed as described in Example 3B. Purification by column chromatography (SiO2, 0-20% methanol/methylene chloride gradient) afforded 25 mg (13%) of the title compound. MS (DCI/NH3) m/z 389 (M+H)+. Anal. Calculated for C22H32N2O2S: C, 68.00; H, 8.30; N, 7.21. Found: C, 67.61; H, 8.67; N, 7.17.

Provenance & Evidence