HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Adamantanecarboxylic acid → HCID 178446104, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Adamantanecarboxylic acid | HCID 13235 | — |
| Reactant | 1-Pentene, 5-bromo- | HCID 70704 | — |
| Reactant | 2-Amino-4,5-dimethyl-1,3-thiazole | HCID 73238 | — |
| Product | HCID 178446104 | HCID 178446104 | — |
Reaction Steps
4,5-Dimethylthiazol-2-ylamine, 5-bromo-pent-1-ene and 1-adamantane carboxylic acid were processed according to the method of Example 47 to afford the title compound. 1H NMR (CDCl3, 500 MHz) δ ppm 1.68 (q, 6 H) 1.74-1.81 (m, 2 H) 1.84 (d, J=2.50 Hz, 6 H) 1.94-2.02 (m, 3 H) 2.10 (q, 2 H) 2.15 (s, 3 H) 2.20 (s, 3 H) 4.11 (t, 2 H) 4.95-5.13 (m, 2 H) 5.80-5.95 (m, 1 H); MS (ESI) m/z 359 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07875639B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-a599c246e461420e8bd43cebad5d405b |
| Source note | uspto-grants-2011_01 |