HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Adamantanecarboxylic acid → HCID 178435122, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Adamantanecarboxylic acid | HCID 13235 | — |
| Reactant | Pentane, 1-bromo-4-methyl- | HCID 69385 | — |
| Reactant | 2-Amino-4,5-dimethyl-1,3-thiazole | HCID 73238 | — |
| Product | HCID 178435122 | HCID 178435122 | — |
Reaction Steps
4,5-Dimethylthiazol-2-ylamine, 1-bromo-4-methyl-pentane and 1-adamantane carboxylic acid were processed according to the method of Example 47 to afford the title compound. 1H NMR (CDCl3, 500 MHz) δ ppm 0.87 (d, J=6.55 Hz, 6 H) 1.18-1.27 (m, 2 H) 1.54-1.62 (m, 1 H) 1.62-1.76 (m, 8 H) 1.84 (d, J=2.50 Hz, 6 H) 1.94-2.03 (m, 3 H) 2.15 (s, 3 H) 2.20 (s, 3 H) 3.98-4.11 (m, 2 H); MS (ESI) m/z 374 (M=H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07875639B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-bc5254b4bd7f4ca4bfa73bc137abdd60 |
| Source note | uspto-grants-2011_01 |