HuagongsheHuagongshe Chemistry Print Report · For research reference only
(1-Bromoethyl)benzene → HCID 178435119, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (1-Bromoethyl)benzene | HCID 11454 | — |
| Reactant | 1-Adamantanecarboxylic acid | HCID 13235 | — |
| Reactant | 2-Amino-4,5-dimethyl-1,3-thiazole | HCID 73238 | — |
| Product | HCID 178435119 | HCID 178435119 | — |
Reaction Steps
4,5-dimethylthiazol-2-ylamine, (1-bromo-ethyl)benzene and 1-adamantane carboxylic acid were processed according to the method of Example 47 to afford the title compound. 1H NMR (CDCl3, 500 MHz) δ ppm 1.51-1.75 (m, 12 H) 1.91 (d, J=6.86 Hz, 6 H) 2.03-2.11 (m, 3 H) 2.14 (s, 3 H) 5.98-6.31 (m, 1 H) 7.21 (d, J=8.11 Hz, 2 H) 7.25 (t, J=7.33 Hz, 1 H) 7.34 (t, J=7.49 Hz, 2 H); MS (ESI) m/z 394 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07875639B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-dfde0ceed50746869fafc7e4ef0d8108 |
| Source note | uspto-grants-2011_01 |