HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiophosgene → [5-(1H-indol-2-yl)-2-methoxy-phenyl]-isothiocyanate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiophosgene | HCID 10040 | — |
| Reactant | 5-(1H-indol-2-yl)-2-methoxy-phenylamine | HCID 9900204 | — |
| Product | [5-(1H-indol-2-yl)-2-methoxy-phenyl]-isothiocyanate | HCID 22568433 | — |
Reaction Steps
The product from Example 1, 5-(1H-indol-2-yl)-2-methoxy-phenylamine, (4.76 g, 20 mmol) was reacted with thiophosgene (1.9 mL, 25 mmol) according to the procedure for Example 23, Step A, to give [5-(1H-indol-2-yl)-2-methoxy-phenyl]-isothiocyanate (4.55 g), as a black solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06858739B2 |
| Source dataset | uspto-grants-2005_02 |
| ORD ID | ord-0fec09881fb740ff8ab79f4f7634b1cd |
| Source note | uspto-grants-2005_02 |