HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromoacetyl bromide → 865106-47-4
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromoacetyl bromide | HCID 61147 | — |
| Reactant | 2-Amino-4,6-difluorophenol | HCID 2737653 | — |
| Reactant | 3-Oxo-3,4-dihydro-2H-benzo[b][1,4]oxazine-6-carbonitrile | HCID 10654813 | — |
| Product | 865106-47-4 | HCID 55252814 | — |
Reaction Steps
Commercially available 2-amino-4,6-difluorophenol (1 g, 6.9 mmol) and bromo acetyl bromide (0.9 mL, 10.3 mmol) were reacted according to the procedure for Intermediate 60 to afford the product as a solid, 208 mg (16%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07875715B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-7f55cde5a5a348ea9761776b44ebb66a |
| Source note | uspto-grants-2011_01 |