HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Isobutylamino-3-nitroquinoline → N4-(2-methylpropyl)quinoline-3,4-diamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Isobutylamino-3-nitroquinoline | HCID 10999310 | — |
| Catalyst | Platinum | HCID 23939 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | N4-(2-methylpropyl)quinoline-3,4-diamine | HCID 11298872 | — |
Reaction Steps
To a solution of 15.0 g (0.0612 mole) of 4-isobutylamino-3-nitroquinoline (from Example 1) in ethanol was added about 0.5 g of 5% platinum on charcoal, and the mixture was hydrogenated on a Parr apparatus at about 20° C. The mixture was filtered to provide a solution of 3-amino-4-(isobutylamino)quinoline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04698348 |
| Source dataset | uspto-grants-1987_10 |
| ORD ID | ord-41d4e2e627904082861cbc2d10ba5a96 |
| Source note | uspto-grants-1987_10 |