Sodium Hydroxide → HCID 23686854, compound

HRID 255597Notes

Reaction equation

HRID 255597 reaction equation
[CH:1]1[CH:2]=[C:3]([C:12]([OH:14])=[O:13])[C:4](=[O:11])[N:5]2[C:10]=1[CH:9]=[CH:8][CH:7]=[CH:6]2.[OH-].[Na+:16]>>[CH:1]1[CH:2]=[C:3]([C:12]([O-:14])=[O:13])[C:4](=[O:11])[N:5]2[C:10]=1[CH:9]=[CH:8][CH:7]=[CH:6]2.[Na+:16]

Participants

3

Reactant 2

HCID 14798Sodium HydroxideHCID 15632080HCID 15632080, compound

Product 1

HCID 23686854HCID 23686854, compound

Procedure

A suspension of 4H-quinolizin-4-one-3-carboxylic acid (196.7 mg) in 0.1N-aqueous sodium hydroxide solution (9.9 ml) was stirred for one hour at room temperature. The resulting reaction mixture was filtered and then the filtrate was lyophilized to give sodium 4H-quinolizin-4-one-3-carboxylate (201 mg).

Workup

  1. customThe resulting reaction mixture
  2. filtrationwas filtered

Sources & evidence

ORD record
ord-913a954439c24f04bd4c5edb585dddcd
Source dataset
uspto-grants-1987_10
Patent number
US04698349

Reaction notes

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