4-Nitrobenzenesulfonyl chloride → HCID 13913718, compound

HRID 255683Notes

Reaction equation

HRID 255683 reaction equation
[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([S:10](Cl)(=[O:12])=[O:11])=[CH:6][CH:5]=1)([O-:3])=[O:2].[CH:14]([NH:17][CH2:18][CH2:19][N:20]([CH:24]([CH3:26])[CH3:25])[CH:21]([CH3:23])[CH3:22])([CH3:16])[CH3:15]>>[CH3:26][CH:24]([N:20]([CH:21]([CH3:23])[CH3:22])[CH2:19][CH2:18][N:17]([CH:14]([CH3:16])[CH3:15])[S:10]([C:7]1[CH:8]=[CH:9][C:4]([N+:1]([O-:3])=[O:2])=[CH:5][CH:6]=1)(=[O:12])=[O:11])[CH3:25]

Participants

3

Reactant 2

HCID 74044-Nitrobenzenesulfonyl chlorideHCID 667971,2-Ethanediamine, N,N,N'-tris(1-methylethyl)-

Product 1

HCID 13913718HCID 13913718, compound

Procedure

p-Nitrobenzenesulfonyl chloride was reacted with N,N',N'-triisopropyl ethylene diamine to obtain the free base of N-[2-[bis(1-methylethyl)amino]ethyl]-N-(1-methylethyl)-4-nitrobenzene sulfonamide as a yellow solid, m.r. 98°-100° C.

Sources & evidence

ORD record
ord-74d683c9e81d48ab893fae832b91766a
Source dataset
uspto-grants-1987_10
Patent number
US04698445

Reaction notes

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