HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-Butyl hypochlorite → 1,1-Di(p-fluorophenyl)-3-chlorourea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-Butyl hypochlorite | HCID 521297 | — |
| Reactant | 1,1-Di(p-fluorophenyl)urea | HCID 13362430 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 1,1-Di(p-fluorophenyl)-3-chlorourea | HCID 20184152 | — |
Reaction Steps
t-Butyl hypochlorite (7.5 g, 0.070 mole) was added to 1,1-di(p-fluorophenyl)urea (17.5 g, 0.071 mole) in 440 ml methanol at 0°-5° and the mixture stirred for 1 hour at that temperature to produce a solution containing step (a) title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04698444 |
| Source dataset | uspto-grants-1987_10 |
| ORD ID | ord-9fb046c3e1464e9dab0c4dd5d80efb9b |
| Source note | uspto-grants-1987_10 |