HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20164527, compound → HCID 20164564, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20164527 | HCID 20164527 | — |
| Solvent | Isoamyl Alcohol | HCID 31260 | — |
| Product | HCID 20164564 | HCID 20164564 | — |
Reaction Steps
Following the procedure described in Example 19 but starting from 1.67 g. of α-(2-carboxyethyl)-mercapto-6,7-dimethoxy-3,4-dihydro-1-isoquinolyl-acetonitrile and 5 ml. of isoamyl alcohol, 1.7 g. of α-[2-(3-methylbutoxycarbonyl)-ethyl]-mercapto-6,7-dimethoxy-3,4-dihydro-1-isoquinolyl-acetonitrile are obtained, melting at 120° C. after recrystallization from isopropanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE032519 |
| Source dataset | uspto-grants-1987_10 |
| ORD ID | ord-4c091ab2deb64994beb98be923fa5604 |
| Source note | uspto-grants-1987_10 |