HCID 13822974, 화합물 → HCID 13923714, 화합물

HRID 255836노트

반응식

HRID 255836 반응식
[Br:1][CH2:2][CH2:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[S:10]([NH:13]C(C)(C)C)(=[O:12])=[O:11]>FC(F)(F)C(O)=O>[Br:1][CH2:2][CH2:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[S:10]([NH2:13])(=[O:11])=[O:12]

참가 물질

3

반응물 1

HCID 13822974HCID 13822974, 화합물

생성물 1

HCID 13923714HCID 13923714, 화합물

시약·촉매·용매 1

HCID 6422Trifluoroacetic acid용매

실험 절차

A solution of 6.3 g of the product from Example 10 in 30 ml trifluoroacetic acid was stirred at room temperature for one hour. The desired product was insoluble in the reaction mixture and was isolated by filtration. Washing with diethyl ether and drying gave 4.5 g of 2-(2-bromoethyl)benzenesulfonamide as a white solid, m.p. 169°-171° C. (dec.).

출처 및 근거

ORD 기록
ord-f79cc49d44514cc795074817fccaedd8
출처 데이터셋
uspto-grants-1987_10
특허 번호
US04699650

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