反应详情

49B was dissolved in 60 ml of toluene containing 5 mg of iodine, and the mixture was refluxed overnight. The solvent was evaporated and the residue was distilled in a short-path bantumware apparatus to give 2-(2-amino-3-methylphenyl)propene (49C), as a colorless oil, b.p.: 82°-85° C. (2 Torr.).

1. temperaturethe mixture was refluxed overnight
2. customThe solvent was evaporated
3. distillationthe residue was distilled in a short-path bantumware apparatus