Isopropylamine → HCID 178457516, compound

HRID 255903Notes

Reaction equation

HRID 255903 reaction equation
C(N[CH:4]=[N:5][C:6]1[CH:11]=[CH:10][C:9]([C:12]2[N:16]=[CH:15][NH:14][N:13]=2)=[CH:8][CH:7]=1)#N.[CH:17]([NH2:20])([CH3:19])[CH3:18]>O>[CH:17]([NH:20][CH:4]=[N:5][C:6]1[CH:11]=[CH:10][C:9]([C:12]2[N:16]=[CH:15][NH:14][N:13]=2)=[CH:8][CH:7]=1)([CH3:19])[CH3:18]

Participants

4

Reactant 2

HCID 6363IsopropylamineHCID 178512243HCID 178512243, compound

Product 1

HCID 178457516HCID 178457516, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

A solution of N-Cyano-N'-[4-(1,2,4-triazol-3-yl)-phenyl]-formamidine (3 g) and isopropylamine (8.5 g) in water (1.5 ml) was stirred for twenty minutes. The crystallized solid was filtered off and purified via its maleate salt in ethanol.

Workup

  1. filtrationThe crystallized solid was filtered off
  2. custompurified via its maleate salt in ethanol

Sources & evidence

ORD record
ord-fe2fe274ad4e4573b6aea4ebe09a8706
Source dataset
uspto-grants-1987_10
Patent number
US04699915

Reaction notes

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