Beta-Alanine → HCID 53738177, compound

HRID 255909Notes

Reaction equation

HRID 255909 reaction equation
[N:1]1([C:6]2[S:10][C:9]([CH:11]=O)=[CH:8][CH:7]=2)[CH:5]=[CH:4][N:3]=[CH:2]1.[N+:13]([CH2:16][CH3:17])([O-:15])=[O:14].NCCC(O)=O>C(O)CCC>[N+:13]([C:16]([CH3:17])=[CH:11][C:9]1[S:10][C:6]([N:1]2[CH:5]=[CH:4][N:3]=[CH:2]2)=[CH:7][CH:8]=1)([O-:15])=[O:14]

Participants

5

Reactant 3

HCID 239Beta-AlanineHCID 6587NitroethaneHCID 133187085-(1H-Imidazol-1-yl)thiophene-2-carbaldehyde

Product 1

HCID 53738177HCID 53738177, compound

Reagents, catalysts & solvents 1

HCID 2631-ButanolSolvent

Procedure

Similar to example 4(a), the reaction is carried out with 60 g 5-(1-imidazolyl)-thiophene-2-aldehyde (EPA No. 112 987), 23.1 g nitroethane, 2 4 g β-alanine and 210 ml n-butanol.

Sources & evidence

ORD record
ord-2543174b4f034a5f8d0dc3341c7826c0
Source dataset
uspto-grants-1987_10
Patent number
US04699914

Reaction notes

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