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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 25597Generated: October 25, 2026

Trifluoroacetic acid → HCID 178457204, compound

https://huagongshe.com/reaction/25597

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
Reactant3-Buten-1-amineHCID 443732—
Reactant4-(Trifluoromethyl)phenyl carbonochloridateHCID 15917597—
ReactantHCID 178484796HCID 178484796—
ProductHCID 178457204HCID 178457204—

Reaction Steps

In analogy to examples 29.10 and 29.11, trans-Methansulfonic acid 5-(4-methyl amino-cyclohexyl)-pentyl ester.trifluoroacetic acid salt and 4-trifluoromethyl-phenyl chloroformate were reacted, followed by treatment with N-allylmethylamine to yield trans-{4-[5-(Allyl-methyl-amino)-pentyl]-cyclohexyl]-methyl-carbamic acid 4-trifluoromethyl-phenyl ester, MS: 441 (MH+).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06858651B2
Source datasetuspto-grants-2005_02
ORD IDord-15b54e768e02409cb2b3fc5755be896d
Source noteuspto-grants-2005_02