HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylhydrazine → t-Butyl alpha-(6-amino-5-oxo-2-phenylperhydro-1,4-thiazepin-4-yl)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylhydrazine | HCID 6061 | — |
| Reactant | t-Butyl alpha-[5-oxo-2-phenyl-6-phthalimidoperhydro-1,4-thiazepin-4-yl]acetate | HCID 20164926 | — |
| Product | t-Butyl alpha-(6-amino-5-oxo-2-phenylperhydro-1,4-thiazepin-4-yl)acetate | HCID 14423825 | — |
Reaction Steps
0.4 g of diastereomer B of t-butyl α-[5-oxo-2-phenyl-6-phthalimidoperhydro-1,4-thiazepin-4-yl]acetate [prepared as described in step (f) above] was subjected to dephthaloylization with methylhydrazine in the same manner as described in Example 1(g), to give 0.22 g of the title compound as an amorphous solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04699905 |
| Source dataset | uspto-grants-1987_10 |
| ORD ID | ord-b963a63bc2de47c0a5d42f61b1530a0f |
| Source note | uspto-grants-1987_10 |