HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 178464452, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | 2-(Ethylamino)ethanol | HCID 8072 | — |
| Reactant | 3,4-Difluorophenyl chloroformate | HCID 22567999 | — |
| Reactant | HCID 178484796 | HCID 178484796 | — |
| Product | HCID 178464452 | HCID 178464452 | — |
Reaction Steps
In analogy to examples 29.10 and 29.11, trans-Methansulfonic acid 5-(4-methyl amino-cyclohexyl)-pentyl ester.trifluoroacetic acid salt and 3,4-difluoro-phenyl chloroformate were reacted, followed by treatment with 2-ethylamino-ethanol to yield trans-(4-{5-[Ethyl-(2-hydroxy-ethyl)-amino]-pentyl}-cyclohexyl)-methyl-carbamic acid 3,4-difluoro-phenyl ester, MS: 427 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06858651B2 |
| Source dataset | uspto-grants-2005_02 |
| ORD ID | ord-5b044c6697134f7598e070df0eb3de79 |
| Source note | uspto-grants-2005_02 |