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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 25603Generated: October 25, 2026

Trifluoroacetic acid → HCID 178457209, compound

https://huagongshe.com/reaction/25603

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
Reactant3-Buten-1-amineHCID 443732—
Reactant4-(Trifluoromethyl)benzenesulfonyl chlorideHCID 2777399—
ReactantHCID 178484796HCID 178484796—
ProductHCID 178457209HCID 178457209—

Reaction Steps

In analogy to examples 29.10 and 29.11, trans-Methansulfonic acid 5-(4-methyl amino-cyclohexyl)-pentyl ester.trifluoroacetic acid salt and 4-(trifluoromethyl)benzenesulphonyl chloride were reacted, followed by treatment with N-allylmethylamine to yield trans-N-{4-[5-(Allyl-methyl-amino)-pentyl]-cyclohexyl}-N-methyl-4-trifluoromethyl-benzenesulfonamide, MS: 461 (MH+).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06858651B2
Source datasetuspto-grants-2005_02
ORD IDord-b16cec55f2074abf9cd51125741926ed
Source noteuspto-grants-2005_02