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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 256038Generated: October 29, 2026

Trifluoroacetic acid → HCID 18610526, compound

https://huagongshe.com/reaction/256038

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 18610543HCID 18610543—
ProductHCID 18610526HCID 1861052692.7%

Reaction Steps

0.41 g of t-butyl α-{6(R)-[1(S)-ethoxycarbonyl-3-phenylpropylamino]-3(R)-methyl-5-oxoperhydro-1,4-thiazepin-4-yl}acetate (isomer B) synthesized as described in Example 30 was subjected to de-t-butylation with trifluoroacetic acid in the same manner as described in Example 3, to give 334 mg of the title compound as an amorphous solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04699905
Source datasetuspto-grants-1987_10
ORD IDord-8aab1ddf2e294fcd8be07b1581d39ca7
Source noteuspto-grants-1987_10