HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 18610526, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 18610543 | HCID 18610543 | — |
| Product | HCID 18610526 | HCID 18610526 | 92.7% |
Reaction Steps
0.41 g of t-butyl α-{6(R)-[1(S)-ethoxycarbonyl-3-phenylpropylamino]-3(R)-methyl-5-oxoperhydro-1,4-thiazepin-4-yl}acetate (isomer B) synthesized as described in Example 30 was subjected to de-t-butylation with trifluoroacetic acid in the same manner as described in Example 3, to give 334 mg of the title compound as an amorphous solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04699905 |
| Source dataset | uspto-grants-1987_10 |
| ORD ID | ord-8aab1ddf2e294fcd8be07b1581d39ca7 |
| Source note | uspto-grants-1987_10 |