HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl bromoacetate → t-Butyl alpha-[2-(2-naphthyl)-5-oxo-6-phthalimidoperhydro-1,4-thiazepin-4-yl]acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl bromoacetate | HCID 79177 | — |
| Reactant | 2-(2-Naphthyl)-5-oxo-6-phthalimidoperhydro-1,4-thiazepine | HCID 20164850 | — |
| Product | t-Butyl alpha-[2-(2-naphthyl)-5-oxo-6-phthalimidoperhydro-1,4-thiazepin-4-yl]acetate | HCID 20164861 | — |
Reaction Steps
4.15 g of 2-(2-naphthyl)-5-oxo-6-phthalimidoperhydro-1,4-thiazepine [prepared as described in step (e) above] were treated with t-butyl bromoacetate in same manner as described in Example 36(f), to give 3.35 g of the title compound as a crystalline solid, melting at 208°-209.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04699905 |
| Source dataset | uspto-grants-1987_10 |
| ORD ID | ord-5987b4a06a514a4f9fecb7f8dccfd7e1 |
| Source note | uspto-grants-1987_10 |