HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-4-hydroxymethyl-3,5,6-trifluoropyridine → HCID 86741835, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-4-hydroxymethyl-3,5,6-trifluoropyridine | HCID 13985161 | — |
| Reactant | cis-3-(2-Chloro-3,3,3-trifluoropropenyl)-2,2-dimethylcyclopropanecarbonyl chloride | HCID 86737382 | — |
| Product | HCID 86741835 | HCID 86741835 | 41.5% |
Reaction Steps
By the method of Example 2, 0.4 g (0.002 mole) of 2-chloro-4-hydroxymethyl-3,5,6-trifluoropyridine (from Example 7) was reacted with 0.54 g (0.002 mole) of cis-3-(2-chloro-3,3,3-trifluoropropenyl)-2,2-dimethylcyclopropanecarbonyl chloride to produce 0.35 g of (2-chloro-3,5,6-trifluoropyridin-4-yl)methyl cis-3-(2-chloro-3,3,3-trifluoropropenyl)-2,2-dimethylcyclopropanecarboxylate as a light yellow oil, Compound 14 in the Tables below.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04701464 |
| Source dataset | uspto-grants-1987_10 |
| ORD ID | ord-ac3d6c141c1a42208c30c2629342029b |
| Source note | uspto-grants-1987_10 |