HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → 1,3-Dihydro-7-(1-pyrrolidinyl)-2H-imidazo-[4,5-b]quinolin-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | 5-[[2-Nitro-5-(1-pyrrolidinyl)phenyl]methylene]-2,4-imidazolidinedione | HCID 53798779 | — |
| Solvent | N,N-dimethylformamide methanol | HCID 21901440 | — |
| Product | 1,3-Dihydro-7-(1-pyrrolidinyl)-2H-imidazo-[4,5-b]quinolin-2-one | HCID 13987617 | — |
Reaction Steps
This compound, m.p. >300° C. (obtained as a dimethylformamide solvate by crystallization from methanol-dimethylformamide), was prepared analogous to Example 4 from 5-[[2-nitro-5-(1-pyrrolidinyl)phenyl]methylene]-2,4-imidazolidinedione.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04701459 |
| Source dataset | uspto-grants-1987_10 |
| ORD ID | ord-f99b9b90d750435d9035d9516f513e49 |
| Source note | uspto-grants-1987_10 |