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HRID256259

反应详情

EQUATION

反应方程式

HRID 256259 的结构方程式

REACTANTS

反应物

2
结构：[BH4-].[Na+]
HCID4311764

Sodium borohydride (Na(BH4))

H4BNa

结构：CC1(C)CCC(C)(C)C1C=O
HCID9793878

Cyclopentanecarboxaldehyde, 2,2,5,5-tetramethyl-

C10H18O

PRODUCTS

生成物

1
结构：CC1(C)CCC(C)(C)C1CO
HCID13629260

(2,2,5,5-Tetramethylcyclopentyl)methanol

C10H20O

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

2,2,5,5-Tetramethylcyclopentane-1-carboxaldehyde is dissolved in 95% ethanol and sodium borohydride is added. After 24 hours, the reaction is quenched with 1M HCl and extracted with ether. The extract is washed, dried over MgSO4 and evaporated to yield 2,2,5,5-tetramethyl-1-cyclopentylmethanol.

WORKUP

后处理

  1. customthe reaction is quenched with 1M HCl
  2. extractionextracted with ether
  3. washThe extract is washed
  4. dry with materialdried over MgSO4
  5. customevaporated