Acetaldehyde → HCID 15159980, compound

HRID 256333Notes

Reaction equation

HRID 256333 reaction equation
[NH2:1][C@@H:2]([C:10]([OH:12])=[O:11])[CH2:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1.[CH:13](=O)[CH:14]([CH3:16])[CH3:15].C(=O)C>>[CH2:13]([NH:1][C@@H:2]([C:10]([OH:12])=[O:11])[CH2:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1)[CH:14]([CH3:16])[CH3:15]

Participants

4

Reactant 3

HCID 177AcetaldehydeHCID 6561IsobutyraldehydeHCID 71567D-Phenylalanine

Product 1

HCID 15159980HCID 15159980, compound

Procedure

Starting from 8.25 g (0.05 mole) of D-phenylalanine, and using the procedure described in Example 3, Step A, except that 9.1 ml (0.1 mole) of isobutyraldehyde are used instead of acetaldehyde, 8.7 g (70%) of the product are obtained.

Workup

  1. customare obtained

Sources & evidence

ORD record
ord-ac30f4b1a883429f82f0a3a08db991fc
Source dataset
uspto-grants-1987_10
Patent number
US04703036

Reaction notes

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