Isobutyraldehyde → HCID 54485855, compound

HRID 256368Notes

Reaction equation

HRID 256368 reaction equation
[NH2:1][CH2:2][C:3]([NH:5][CH2:6][C:7]([NH:9][CH2:10][C:11]([N:13]1[CH2:17][C:16](=[O:18])[NH:15][C:14]1([CH3:20])[CH3:19])=[O:12])=[O:8])=[O:4].[CH:21](=O)[CH:22]([CH3:24])[CH3:23]>CO>[CH3:19][C:14]1([CH3:20])[NH:15][C:16](=[O:18])[CH2:17][N:13]1[C:11](=[O:12])[CH2:10][NH:9][C:7](=[O:8])[CH2:6][N:5]1[C:3](=[O:4])[CH2:2][NH:1][CH:21]1[CH:22]([CH3:24])[CH3:23]

Participants

4

Reactant 2

HCID 6561IsobutyraldehydeHCID 20163749HCID 20163749, compound

Product 1

HCID 54485855HCID 54485855, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

A solution of 1-[2-[2-(2-aminoacetamido)acetamido]acetyl]-2,2-dimethyl-4-imidazolidinone (0.5 g) and isobutyraldehyde (0.18 ml) in methanol (5 ml) was refluxed for 0.5 hours.

Sources & evidence

ORD record
ord-279abe9173b144ac8fd36f3acc8b47f6
Source dataset
uspto-grants-1987_10
Patent number
US04703054

Reaction notes

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