Triethylamine → HCID 13728729, compound

Participants

Reaction Steps

A mixture of 13 g (0.0289 mole) of the above product, 8.77 g triethylamine and 4.66 g (0.0318 mole) cyclohexylcarbonyl chloride and 120 ml toluene was heated at reflux under nitrogen for six hours, cooled, filtered to remove insoluble matter and the filtrate concentrated in vacuo. The residual solid was flash chromatographed, eluting with hexane to obtain 4.7 g (81%) of white crystals, m.p. 32°-34° C. Mass spectrum (m/e): 200 (M+).

Provenance & Evidence