HuagongsheHuagongshe Chemistry Print Report · For research reference only
o-Xylyl bromide → HCID 21279347, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | o-Xylyl bromide | HCID 6992 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 21279347 | HCID 21279347 | 58.2% |
Reaction Steps
The procedure of Example 1 is repeated using 21.2 g of sodium carbonate, 3.47 g of hydroxylamine hydrochloride and 18.51 g o-methylbenzyl bromide in 75 ml of dimethylformamide. Recrystallization from ethanol affords 7.01 g of the title hydroxylamine as a white solid, mp 90°-93° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04703073 |
| Source dataset | uspto-grants-1987_10 |
| ORD ID | ord-cdb6b6302e774d3fa134c729d94580e9 |
| Source note | uspto-grants-1987_10 |