HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → HCID 20163824, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | 1-(Chloromethyl)-4-dodecylbenzene | HCID 14385728 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 20163824 | HCID 20163824 | — |
Reaction Steps
The procedure of Example 1 is repeated using 16.0 g of sodium carbonate, 2.57 g of hydroxylamine hydrochloride and 21.83 g of p-dodecylbenzyl chloride in 75 ml of dimethylformamide kept at 50°-55° C. overnight under nitrogen. The product is isolated as a light brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04703073 |
| Source dataset | uspto-grants-1987_10 |
| ORD ID | ord-99fb2909f79445eead3763d08521b4d9 |
| Source note | uspto-grants-1987_10 |