Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2,6-Diethylaniline | HCID 11369 | — |
| Solvent | Water | HCID 962 | — |
| Product | 7-Ethylindole | HCID 2724711 | 41% |
Reaction Steps
The reactor filed with Cu-chromite/BaO catalyst was heated to 610° C. Into the reactor was fed 68.4 g of 2.6-diethylaniline and 41.4 g of water per hour. The organic reaction product after 5 hours of such reaction conditions was collected and subjected to partial hydrogenation as described in Example 1. After filtering of the hydrogenation catalyst, 332.4 g of organic liquid containing 45.8 g percent of 2.6-diethylaniline and 41.0 percent of 7-ethyl indole was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04703126 |
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| Source dataset | uspto-grants-1987_10 |
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| ORD ID | ord-5f61a3c7d5a542b78f62338db1c14ba5 |
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| Source note | uspto-grants-1987_10 |
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