HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 19785474, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 19785494 | HCID 19785494 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 19785474 | HCID 19785474 | — |
Reaction Steps
4-[(1-azabicyclo[2.2.2]oct-3-yl)oxy]benzenamine (Example 3) was acetylated with acetic anhydride in dry pyridine at -10° C. The crude product was converted into the hydrochloric salt to obtain N-[4-[(1-azabicyclo[2.2.2]-oct-3-yl)oxy]phenyl]acetamide hydrochloride. M.p. >250° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05258392 |
| Source dataset | uspto-grants-1993_11 |
| ORD ID | ord-a68130013335449db4b8ecfabc11a40b |
| Source note | uspto-grants-1993_11 |