HCID 135588842, compound → HCID 178457752, compound

HRID 256818Notes

Reaction equation

HRID 256818 reaction equation
[N+:1]([C:4]1[NH:8][CH:7]=[N:6][C:5]=1[C:9](=[O:14])[NH:10][CH2:11][CH:12]=[CH2:13])([O-])=O>[Cl-].[Cl-].[Ti+2]>[NH2:1][C:4]1[NH:8][CH:7]=[N:6][C:5]=1[C:9](=[O:14])[NH:10][CH2:11][CH:12]=[CH2:13]

Participants

3

Reactant 1

HCID 135588842HCID 135588842, compound

Product 1

HCID 178457752HCID 178457752, compound

Reagents, catalysts & solvents 1

HCID 10290777Titanium(2+);dichlorideCatalyst

Procedure

The 5-amino-4-allylcarbamoylimidazole was prepared from 5-nitro-4- allylcarbamoylimidazole (m.p. 218°-220C.) by reduction by means of titanous chloride.

Sources & evidence

ORD record
ord-9297cf0bc96e438b967ffee78a4a41d0
Source dataset
uspto-grants-1993_11
Patent number
US05260291

Reaction notes

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