HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 131988-12-0
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Pyridine, 3-(4-ethoxy-1,2,5-thiadiazol-3-yl)- (9CI) | HCID 15180131 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 131988-12-0 | HCID 15819042 | — |
Reaction Steps
A mixture of methyl iodide (0.3 ml, 5 mmol) and 3-(4-ethoxy-1,2,5-thiadiazol-3-yl)pyridine (520 mg, 2.5 mmol) in acetone (10 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.72 g (83%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05260311 |
| Source dataset | uspto-grants-1993_11 |
| ORD ID | ord-c6ef184dca474ec6ac95906eed20063b |
| Source note | uspto-grants-1993_11 |