HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 256934Generated: October 30, 2026
Isoamyl Alcohol → HCID 19075319, compound
https://huagongshe.com/reaction/256934
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Isoamyl Alcohol | HCID 31260 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | 3-Chloro-4-(pyridin-3-yl)-1,2,5-thiadiazole | HCID 10488164 | — |
| Product | HCID 19075319 | HCID 19075319 | — |
Reaction Steps
To a solution of sodium (230 mg, 10 mmol) in isopentanol (20 ml) was added 3-(4-chloro-1,2,5-thiadiazol-3-yl)pyridine (490 mg, 2.5 mmol). The mixture was stirred at 50° C. for 2 h and evaporated. The residue was dissolved in water and extracted with ether. The combined organic phases were dried and evaporated to give the wanted compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05260311 |
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| Source dataset | uspto-grants-1993_11 |
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| ORD ID | ord-526e53e7345045818e5a2125ed9dcb8e |
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| Source note | uspto-grants-1993_11 |
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