Methyl iodide → HCID 19075363, compound

HRID 256935Notes

Reaction equation

HRID 256935 reaction equation
[CH3:1][I:2].[CH2:3]([O:8][C:9]1[C:10]([C:14]2[CH:15]=[N:16][CH:17]=[CH:18][CH:19]=2)=[N:11][S:12][N:13]=1)[CH2:4][CH:5]([CH3:7])[CH3:6]>CC(C)=O>[I-:2].[CH2:3]([O:8][C:9]1[C:10]([C:14]2[CH:15]=[N+:16]([CH3:1])[CH:17]=[CH:18][CH:19]=2)=[N:11][S:12][N:13]=1)[CH2:4][CH:5]([CH3:7])[CH3:6]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 19075319HCID 19075319, compound

Product 1

HCID 19075363HCID 19075363, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.5 ml, 10 mmol) and 3-(4-isopentyloxy-1,2,5-thiadiazol-3-yl)pyridine (622 mg, 2.5 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.78 g (81%).

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 0.78 g (81%)

Sources & evidence

ORD record
ord-2f99eaae2e574d27924211dcd61b860d
Source dataset
uspto-grants-1993_11
Patent number
US05260311

Reaction notes

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