Methyl iodide → HCID 19075430, compound

HRID 257017Notes

Reaction equation

HRID 257017 reaction equation
[CH3:1][I:2].[CH2:3]([S:11][C:12]1[C:13]([C:17]2[CH:18]=[N:19][CH:20]=[CH:21][CH:22]=2)=[N:14][S:15][N:16]=1)[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10]>>[I-:2].[CH2:3]([S:11][C:12]1[C:13]([C:17]2[CH:18]=[N+:19]([CH3:1])[CH:20]=[CH:21][CH:22]=2)=[N:14][S:15][N:16]=1)[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10]

Participants

3

Reactant 2

HCID 6328Methyl iodideHCID 15180158HCID 15180158, compound

Product 1

HCID 19075430HCID 19075430, compound

Procedure

Methyl iodide (0.5 ml, 7.5 mmol) was added to a solution of 3-(4-octylthio-1,2,5-thiadiazol-3-yl)pyridine (3 mmol) and the reaction mixture was stirred at room temperature for 48 h and evaporated.

Workup

  1. customevaporated

Sources & evidence

ORD record
ord-652b66c057b042ef95201a095f11252e
Source dataset
uspto-grants-1993_11
Patent number
US05260311

Reaction notes

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